MPFREE

The MPFREE Standard

Every number on this page ships with a dated rationale document and an effective date — see §2b of the architecture spec. Until the Scientific Advisory Board publishes a threshold for a given matrix and method, this page shows no invented number for it. What follows below is real: the analytical methods, their size floors and units, and the full matrix of matrices and methods this Standard covers — sourced from the current published literature, not from marketing copy.

Pillar 1 — Ingestion & In-Use Risk

Inside the product

Liquid, food contents, active crop tissue, and primary product formulation. Must test below the current SAB-published threshold for the applicable matrix, using µFTIR, Raman microspectroscopy, and/or Py-GC-MS as specified per method below.

Pillar 2 — Environmental Impact

Downstream waste

Farm mulches, processing effluent, primary/secondary packaging. No persistent synthetic polymer content, verified by material composition audit; degradability claims require independent third-party test data.

Detection methods

A microplastic is currently defined, under the cross-matrix framework this Standard follows, as a solid, water-insoluble plastic particle with at least one dimension between 1 µm and 1,000 µm [1]. No single method covers that whole range with one output type, which is why three methods are required rather than one.

µFTIR

Particle count and polymer identity via infrared spectral matching. Conventional practical size floor ≈ 20 µm [2]; specialized large-area ATR variants have reached ≈1.3 µm in research settings, though not yet at routine accredited-lab scale [3].

Raman microspectroscopy

Particle count and polymer identity via inelastic light scattering. Practical size floor ≈1 µm — an order of magnitude finer than conventional µFTIR [4].

Py-GC-MS

Total polymer mass via pyrolysis and mass spectrometry — reported down to nanogram levels across common polymers [5]. Destroys the sample, so it produces no particle size, shape, or count data [6] — but has no size floor at all, which is what makes it the only method here that captures the sub-1-µm nanoplastic fraction neither optical method can resolve.

Published thresholds

Agricultural Produce

Py-GC-MS
mass basis, no size floor · ug_per_kg
Pending SAB determination
Rationale →
Raman microspectroscopy
size floor ≈ 1.000 µm · particles_per_kg
Pending SAB determination
Rationale →
µFTIR
size floor ≈ 20.000 µm · particles_per_kg
Pending SAB determination
Rationale →

Beverages

µFTIR
size floor ≈ 20.000 µm · particles_per_L
Pending SAB determination
Rationale →
Raman microspectroscopy
size floor ≈ 1.000 µm · particles_per_L
Pending SAB determination
Rationale →
Py-GC-MS
mass basis, no size floor · ug_per_kg
Pending SAB determination
Rationale →

Solid & Packaged Foods

Py-GC-MS
mass basis, no size floor · ug_per_kg
Pending SAB determination
Rationale →
Raman microspectroscopy
size floor ≈ 1.000 µm · particles_per_kg
Pending SAB determination
Rationale →
µFTIR
size floor ≈ 20.000 µm · particles_per_kg
Pending SAB determination
Rationale →

This isn't just internal caution: the WHO's 2019 review of microplastics in drinking water explicitly called for standardized measurement methods as a precondition for a more confident risk assessment [7] — the methods above are that standardization in progress, and the numeric column reflects that it isn't finished yet.

Accredited laboratory network

Example Analytical Labs (DEMO)
ISO/IEC 17025 — A2LA (placeholder) · scope →

Scientific Advisory Board

Not yet constituted. Per §2b, this Standard requires the SAB to be independent (majority non-employee, published conflict-of-interest disclosures, no member setting a threshold for a certification they also audit) before it may publish a single numeric limit — that's a deliberate sequencing choice, not an oversight. Roster and disclosures will be published here once the board is seated; until then, the pending state in the table above is the accurate, honest status.

Accreditation status

ISO/IEC 17065 (certification body) — accreditation in progress. Partner labs above already hold ISO/IEC 17025 accreditation for the methods listed.

Sources

  1. [1] ISO 24187:2023. "Principles for the analysis of microplastics present in the environment." International Organization for Standardization. View source →
  2. [2] ACS Omega (2022). "Detection of Sub-20 μm Microplastic Particles by Attenuated Total Reflection Fourier Transform Infrared Spectroscopy and Comparison with Raman Spectroscopy." View source →
  3. [3] Marine Pollution Bulletin (2023). "Detecting small microplastics down to 1.3 μm using large area ATR-FTIR." View source →
  4. [4] PMC (2023). "TUM-ParticleTyper 2: automated quantitative analysis of (microplastic) particles and fibers down to 1 μm by Raman microspectroscopy." View source →
  5. [5] PMC (2024). "Rapid and Sensitive Quantification of Nano- and Microplastics in Water, Sediment, and Biological Tissue by Pyrolysis-Gas Chromatography Tandem Mass Spectrometry with Dynamic Reaction Monitoring." View source →
  6. [6] PMC (2023). "Analysis of microplastics in the environment: Identification and quantification of trace levels of common types of plastic polymers using pyrolysis-GC/MS." View source →
  7. [7] World Health Organization (2019). "Microplastics in Drinking-Water." View source →